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Poor Conversion

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  • Poor Conversion

    Hi again, i just did a 60 litre batch and after the conversion rate test (brilliant) got the bad news that it was not a particlarly good conversion, now, as i am 99% sure that i used enough KOH (this time), i was wondering what other factors could contribute to the poor conversion.. and what should i do with it now? is it still usable, or should i reprocess it?
    i am champion at making 1 litre batches,..hah.. they turn out really well, mabey i should make lots and lots of them eh?
    thanks

  • #2
    Re: Poor Conversion

    ok there it is

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    • #3
      Re: Poor Conversion

      Hello Eddie,

      Poor conversion can be caused by,

      Not enough NaOH/KOH
      Poor quality NaOH/KOH
      Not enough methanol
      Poor quality methanol
      Not enough time mixing for the temperature the reaction is performed at..
      Poor quality mixing equipment.
      Too much water in the reaction.

      Tilly

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      • #4
        Re: Poor Conversion

        ok thanks tilly, the fact that my one litre batches work well leads me to think its prolly the reactor, or not enough mixing perhaps. i will modify a few bits and try again.. and again.. hah.

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