Tried my first mix, 200 litres of oil. titration worked out to 1600 gms koh in 40 litres methanol. mixed it for an hour at 50 degrees but no separation.
Did another test on the mixture in processor and it looks like I was to hasty with the first titration.
The new titration calls for 1800 gms koh.
Question is -- can I restart the reaction?
A friend suggestion I just treat it as a new mix but do I need to add another 40 litres of methanol or do I use a small amount of methanol with 1800 grams of koh?
Any help would be much appreciated.
Did another test on the mixture in processor and it looks like I was to hasty with the first titration.
The new titration calls for 1800 gms koh.
Question is -- can I restart the reaction?
A friend suggestion I just treat it as a new mix but do I need to add another 40 litres of methanol or do I use a small amount of methanol with 1800 grams of koh?
Any help would be much appreciated.
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